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Protamine

Overview

Field Detail
Drug class Heparin reversal agent
Route IV
Stock formulation 50 mg/5 mL
Reconstituted conc. N/A (10 mg/mL ready to use)
Diluent Nil
Storage Refrigerate 2–8 °C; do not freeze

Preparation

Before you start

Check the expiry date and vial integrity before opening. Label every syringe immediately after drawing up — never leave unlabelled syringes on the tray.

Equipment needed

  • 1 × Protamine 50 mg/5 mL (10 mg/mL) vial
  • Normal saline (NS) — for IDT dilutions
  • 1 mL syringes × 3
  • 25 G needles

Step 1 — Prepare the SPT solution (10 mg/mL — neat)

  1. Draw up 0.5–1 mL of the stock (10 mg/mL) into a 1 mL syringe.
  2. Label: "Protamine SPT 10 mg/mL".

Step 2 — Prepare IDT dilutions

Prepare in this order, using a fresh syringe for each step.

  1. IDT 0.01 mg/mL (1:1,000):

    • Draw 0.1 mL of stock (10 mg/mL) into a 1 mL syringe. Add 0.9 mL NS. Mix. (This is 1 mg/mL — 1:10).
    • Draw 0.1 mL of this 1 mg/mL into a new 1 mL syringe. Add 0.9 mL NS. Mix. (This is 0.01 mg/mL — 1:1,000).
    • Label: "Protamine IDT 0.01 mg/mL".
  2. IDT 0.05 mg/mL (0.1:20):

    • Draw 0.1 mL of stock (10 mg/mL) into a 1 mL syringe. Add 1.9 mL NS. Mix. (This is 0.05 mg/mL — 0.1:20).
    • Label: "Protamine IDT 0.05 mg/mL".

Unusual dilution

The 0.1:20 dilution for Step 2 is non-standard. Ensure accuracy when measuring 0.1 mL stock + 1.9 mL NS.


Skin prick test (SPT)

Reagent Concentration
Test solution Neat (10 mg/mL)
Positive control Histamine 10 mg/mL
Negative control Normal saline

Interpretation: Wheal ≥3 mm vs negative control = positive.


Intradermal test (IDT)

Dilution series

Step Dilution Concentration Preparation
1 1:1,000 0.01 mg/mL 0.1 mL of 1 mg/mL + 0.9 mL NS
2 0.1:20 0.05 mg/mL 0.1 mL of 10 mg/mL + 1.9 mL NS

Inject: 0.05 mL intradermal. Read at 15–20 minutes.